stpug
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Here's results from a new experiment. I bought a refractometer so I could grab samples on the fly without waiting 10 minutes for them to cool. Mash temperature for this batch was 154F. which seemed like a good temperature for a sweet stout and it's in the range where conversion should happen rapidly. I did not do an iodine test during this mash, I forgot about that until just now.
Time Gravity
5 minutes 1.015
10 minutes 1.017
stirred mash
11 minutes 1.026
stirred mash
15 minutes 1.033
stirred mash
20 minutes 1.040
stirred mash
25 minutes 1.047
stirred mash
30 minutes 1.051
stirred mash
35 minutes 1.048
stirred mash
40 minutes 1.051
Looking through the numbers, it appears that the 30 minute sample was an error and that there was some but minimal increase between 25 and 40 minutes. This needs to be run again to see if the results are consistent but for a preliminary result, 20 to 25 minutes is the sweet spot. Longer is better but not by much. Now for the fermentability, which will have to wait for this batch.
A previous batch of blonde ale using Danstar Windsor yeast had an OG (hydrometer) of 1.040 and at 2 weeks it has come down to 1.008, and 80% attenuation for a yeast that should attenuate 62 to 68%. This batch was mashed at 156F for 20 minutes and hot water was used for sparging to get my volume because the pot I used was too small to go full volume.
A few observations on your experiment:
-Careful of overheating the crystal on your refract. Once the crystal gets overheated then it can produce wonky results for longer than expected (i.e. until the crystal cools back down to within calibration range).
-Careful of overcooling the crystal for the same reason.
-Try to put lightly warm wort on a room temp crystal and rinse with room temp water.
-When we are talking about "complete/full" conversion we are looking for the point at which the gravity no longer continues to rise (right?), and if you think the 30 minute reading is unreliable (i.e. toss it out) then technically you never reached the point at which the gravity was no longer rising. I, on the other hand, suspect the 35 minute reading is wonky which would mean the readings between 30 and 40 remained the same to indicate full conversion. In other words, I would call the "sweet spot" (literally) at 30 minutes, which is within reason for a 154 mash temp using well crushed grain.
-As for attenuation levels from various yeast strains, we gotta call a meeting with those strains because the ranges manufacturers are supplying us with are generally piss poor