Does anyone have the ASBC Methods of Analysis CD or book? If so, can I rent it from you for a while?
Which ones in particular? I don't have them, but you will need to be specific.
2009 is going to be hard to find given the price. And obviously they will not be able to rent them out due to license reasons.
The MOA are really just a standardized industry test so that you can take the results and compare them over years and between breweries.
In my old age I have become more observant of the ethics involved in such things. I think it all came home to me on the day a friend got quite PO'd when my son suggested he was going to make a copy of the $15 music CD his wife peddles. This was, and you probably know this is coming, the same guy that wanted me to copy Adobe Photoshop for him (or buy him a bootleg copy in Bangkok or something similar). I've got qualms with respect to the ASBC because they are a not for profit organization. Their lifeblood is dues and what they can get for selling publications, check services etc.
Yes, that is the intent but the industry is the brewing industry. The paint industry does not measure color the way the brewing industry does. The only place where there is 100% cross over is with respect to water chemistry. There are no water chemistry methods in the MOAs. Standard Methods for the Analysis of Water and Waste Water (developed for the drinking water and sewage treatment industries) is incorporated by reference. You can probably find that in libraries. Yes, the test for protein is basically a Kjeldahl test but it has been tweaked for beer/wort. Of course if you are only interested in knowing how to test for protein using Kjeldahl's method you can look it up o Wikipedia.
Now if you are interested in one or 2 I wouldn't have a problem sending those to you (reasoning that the ASBC isn't going to get your money in any case) but I wouldn't feel right about flagrantly violating the license agreement.
Another suggestion you might want to consider: they also publish "Laboratory Methods for Craft Brewers". As the name suggests it is not nearly as extensive (or expensive) as the full set of MOAs and contains all the methods that a home brewer is ever going to contemplate.
I'd also be happy to tell you about what's involved in carrying out any of the analyses that I know about (i.e. the ones I've done).
mjc1024 said:Hey, I'm interested in getting some of the ASBC methods of analysis. Do you still have them available?
That's more like it.You're right, I shouldn't be discouraging. I may have been. I originally started this lab far before we were brewing and I had purchased a lot of used stuff on ebay, and most of it is in production today. A GC can be had for under $2k, UV/VIS under $500, and a wrist action shaker for about a hundred bucks (we used to shake our vials by hand). Chinese glassware might be had for $1000 or less and a good microscope from ebay for less than $300. We had a $200 ebay centrifuge, it only held 15ml vials, and repeatability was below useful. The Anton Paars are $30-$60k our density/alcohol meter is made by Mettler Toledo and saved us $20k. Most of the instruments aren't inheriently expensive. We have expensive and cheap instruments and that's not where the trouble lies.
No disagreement there. In my experience if you do a couple by hand you'll be happy to shell out for the shaker and repeatability is frosting on the cake.Your dude, shaking his vials might be an expert, but he's just not going to shake that stuff the same every time.
The IBU method already has problems with dissolved particulates without standardized shaking.
The diacetyl method you mention, to be fair, only measures total vicinal
diketones, you really need a GC to measure diacetyl. The method for Diacetyl UV/VIS (from 1964) was archived in 1992. I'm not sure why they archive the methods, but it's accuracy is questionable, given the requirements for tenths of a milligram weights and internal standards and all that. Not saying it can't be done, it will take loads of discipline to accomplish accurately.
Wow. You don't mean that. An ABV report of 5 ± 2% would be pretty useless data almost 2 orders of magnitude worse than I can do as a 'kitchen chemist'. I've done error analysis on my ethanol recovery and have a total error budget of 0.03% for a beer with 10% ABV. I think you must have meant 2% CV e.g if the beer were 10% the error would be 0.02*10 = ±0.2% ABV.I'm just saying, I don't think people should get their hopes up about being able to these analysis with accuracy. I'd say ±10 IBU, ±2% abv
I'm looking for a sample of the ICE-3 calibration standard for HPLC analysis. I just want to do a single AA analysis on the hops I picked this fall but I can't justify buying the whole sample for $150 for only 3 analyses.
We do still have them. They are kept online and protected by a password and ASBC.org asks for our IP address to allow it through their firewall. There are hundreds and hundreds, maybe thousands of methods. You'll have to know the specific method you'd like to perform and I'll happily discuss how we perform the method in our lab and how you might want to achieve the same things in yours.
The diacetyl method you mention, to be fair, only measures total vicinal
diketones, you really need a GC to measure diacetyl.
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