The weather warmed up enough here that I was able to get two batches in over the last two days. This time I made sure to stir the mash well prior to taking any samples.
Sticking with my Zombie Dust clone, and a target of 5.25 gallons into the fermenter for both batches.
10.24 lb Great Western Organic 2-Row
1.05 lb American Munich (10L)
0.42 lb CaraFoam
0.42 lb Crystal 60
0.42 lb Melanoidin
Total grain bill: 12.55 lb
Starting water volume: 8.4 gallons
Target OG: 1.065
Mash temp: 152F
Batch #1: mill gap set to 0.025"
I refired the burner at 15, 30, and 45 minutes
Mash:
15 min: 151F, 8.3 brix refractometer, pH 5.24
30 min: 151F, 10.0 brix refractometer, 10.3 brix hydrometer
45 min: 151.4F, 10.9 brix refractometer, pH 5.27
60 min: 151.5F, 11.5 brix refractometer
post-squeeze: 11.5 brix refractometer
Conversion efficiency per Braukaiser formula: 90.7%
Volume after boil and chilling wort: 6 gallons
I was barely able to collect my 5.25 gallons, with about .75 gallons left in the kettle which was composed mostly of hop leaf, plus maybe a pint of wort.
After chilling wort: 14.2 brix refractometer, 14.0 brix hydrometer
Batch #2: mill gap set to 0.022"
I refired the burner at 15 and 45 minutes (must not have stirred well enough while reheating at 15 minutes, as it was still above target temp at 30 minutes)
Mash:
15 min: 150.4F 11.3 brix refractometer, pH 5.31
30 min: 153.0F, 10.6 brix refractometer, 11.0 hydrometer - not sure why I went backwards here
45 min: 150.6F, 11.3 brix refractometer
60 min: 11.9 brix refractometer
Conversion efficiency per Braukaiser: 94.3%
Volume after boil and chilling wort: 5.75 gallons (more vigorous boil for this batch)
I used pellet hops for this batch rather than whole leaf, and was easily able to collect my target volume with some left over in the kettle, probably because with pellet hops most of them get sucked into the fermenter.
After chilling wort: 15.3 brix refractometer, 15.3 brix hydrometer
Some observations:
- I try to take all measurements with the wort temperature within 1 degree of 20C. A hydrometer tube sample takes some time to cool, and I then pull the refractometer sample from the top of the hydrometer tube. I almost always get a lower reading on my refractometer doing this, likely because while the tube is sitting to cool, more sugary dense wort collects near the bottom, so the refractomer sample I pull from the top reads lower. When I take a hydrometer sample after boiling and chilling the wort with my immersion chiller, I don't have to wait for the sample to cool, so there is less chance for stratification within the hydrometer tube. I find I get very similar readings between my refractometer and hydrometer on these measurements. In the future if I pour the hydrometer tube into a second vessel prior to pulling a refractometer sample, I may see more consistent results.
- There appears to be some disagreement on brix to SG conversion.
BYO cites this formula as the most accurate. The same formula is referenced
here:
SG = 1.000019 + [0.003865613(brix) + 0.00001296425(brix) + 0.00000005701128(brix)]
Taking the OG from my second batch, this formula says 15.3 brix = 1.059 SG. I believe this formula is accounting for a wort correction factor of 1.04.
On a
different page, BYO cites a different formula:
{Plato/(258.6-([Plato/258.2]*227.1)}+1 = Specific gravity
This formula says 15.3 brix = 1.062 SG
This calculator uses an iterative technique to convert between the two:
Its calculator says 15.3 brix = 1.062 SG
Most conversions seem to put 15.3 brix at 1.062 SG, so I'm going with that
edit - lots of good information on the various ways to convert between brix and sg here.
- I wonder how much volume loss occurs during mash. There is a decent amount of evaporation happening, and when stirring the wort and taking measurements, the lid is off allowing some to escape. If the amount lost is significant, that would mean my conversion efficiency measurements are on the generous side.
- When boiling the second batch, I noticed that by the end of 60 minutes my boil was not nearly as vigorous as at the start. I would think that as the volume decreases, it would be easier to maintain a vigorous boil, as I had my propane burner turned on full blast for the full 60 minutes. I still have about a quarter of a tank left, but it could be lower pressure out of the tank as it runs lower. I'm not sure how to solve this without the inconvenience of not using the second half of a propane tank for brewing. Another explanation is that as the density of the wort increases, so does its boiling point.
- Brewer's Friend appears to have corrected the conversion efficiency calculation in their
Brew Session tool. Their
brewhouse efficiency calculator still reports a different result. For batch #1 I calculated a conversion efficiency of 90.7% using Braukaiser's formula. Brewer's Friend's Brew Session tool reports 91% conversion efficiency. Their brewhouse efficiency calculator reports 83% with the same inputs.