refractometer accuracy

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Hoochin'Hank

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If my refractometer has been spot-on with my hydrometer for over a dozen beers (most were between 1.050 and 1.065), is there any reason to doubt it's accuracy on a real heavy (1.100) wort?
 
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Hoochin'Hank

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The refractometer claims it does auto temp correction, altho it doesn't exactly take more than a minute for the couple drops to cool to room temperature (the whole wort is already down to 83F). But my hydrometer only goes up to 1.070, so I can't double-check. I only ask, because my gravity came in a little lower than expected (1.088 vs 1.101) on an extract batch.
 

BrewZer

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It's prob'ly accurate enough for homebrewer work. Gravity can shift down if you don't get as much water boiling off or you added not quite as much LME or adjunct sugar as your recipe suggests.

Did you scrape out those cans like they owed you money? Did you weigh out your sugar vs. use a volumetric measure? Those things can throw off the figures by a few points.
 
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Hoochin'Hank

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That's why I was questioning if the refractometer maybe gets a little less accurate at higher gravities... I suppose if I dilute my hydro sample with equal parts water (hmm, by weight? or by volume?) I should be able to get a good hydrometer reading...

Then again, I had a lot more steeping grain and hops (than I usually use) that surely soaked up some wort, that likely got replaced with top-off water.
 

NSMikeD

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Yes, a hydrometer becomes less accurate as it measures liquids that move away from where it was calibrated. Perhaps not as much as what you're experiencing. Also. keep in mind that temperature affects readings for both hydrometers and refractometers and automatic corrections are not always precise, again, less so as you move away from room temperature.

fwiw, whenever I get a questionably reading I usually attribute it to user error which almost always is confirmed weeks later by my taste buds.
 

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I have a pretty cheap refractometer, and recently it was giving inaccurate results. I finally figured out what happened. When washing it off, some water slipped past the glass and was inside of the unit. I was able to wick it all out with a dry towel and the accuracy I used to have came back.
 
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my gravity came in a little lower than expected (1.088 vs 1.101) on an extract batch.
Without supporting information, an OG miss of this size could be due to a missing ingredient; but ...

I had a lot more steeping grain and hops (than I usually use) that surely soaked up some wort, that likely got replaced with top-off water.
... with top-off water, stratification is a likely cause as well.

I suppose if I dilute my hydro sample with equal parts water (hmm, by weight? or by volume?) I should be able to get a good hydrometer reading...
Measuring the dilution will need some precise measurements. Maybe measuring dilution by weight and volume would be a good cross-check.

Another approach might be to build a solution using simple sugar; take an SG measurements for solutions at around OG 50, 70, 90, 110.

There are some additional ideas in the /r/homebrewing wiki refractometer page.
 
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Hoochin'Hank

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Measuring the dilution will need some precise measurements. Maybe measuring dilution by weight and volume would be a good cross-check.
Since the hydrometer is measuring the amount of sugar in a specific VOLUME, I think diluting with equal parts by volume would have to be the way to go.

Another approach might be to build a solution using simple sugar; take an SG measurements for solutions at around OG 50, 70, 90, 110.
I've decided to just leave it be, it'll just be touch lighter on the ABV*. Now, if that whole pack of US-05 I added about 12 hours ago would stop slouching and ACT BUSY, I'd be so much less worried!

*say, that'd leave space for a little bourbon flavor...
 

AZ Maverick

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If you want to check your refractometer at the high end you can make a sugar solution to test it.
I zero tare a small container on my kitchen scale then add 14 grams of table sugar and then add water until the scale reads 50 grams and then mix it very well - that is a 28% sugar solution (or 28 Plato). 28 Plato is 29.1 brix or 1.120 SG.
My ATC refractometer reads in brix and is dead on 29.1 brix with the above 28% sugar solution.
 
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Hoochin'Hank

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*say, that'd leave space for a little bourbon flavor...
Beer went from 1.088 down to 1.015 (so 9.5% abv), and has been sitting there for over a week. I've got about 2.8 gallons to bottle (guesstimating, not quite sure how deep the yeast cake is). Is there any kind of rule-of-thumb for ounces of bourbon to add to one gallon? I know the usual suggestion of dosing a small sample until the taste is good, and then scaling that up -- but that's not terribly practical when the beer still has a good hop burn and zero carbonation.
 

z-bob

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I've had problems with my refractometer occasionally reading really low; like 7 brix when it's really 11 or 12. I'll double-check it and get the same reading. I messed up one beer (didn't quite ruin it) by adding a pound of DME and the beer didn't have that much hops to balance it. I think what is happening is a little bit of grist is getting on the glass so the coverplate isn't sitting level. I'll have to watch for that.
 
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Hoochin'Hank

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well if the refrac was right, it should read 10.5 now?
and that gravity i'm assuming was corrected right?
I'd have sworn I'd recorded the original brix reading when I brewed this, but I can't find my notes on this one, so all I've got to go off is this forum thread, where post #3 says I got 1.088 (I always use Refractometer Calculator - Brewer's Friend with a 1.04 wcf). Anyways, it was a DME extract batch, and I'm quite certain the "miss" was adding too much top-off water.
 

bracconiere

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I'd have sworn I'd recorded the original brix reading when I brewed this, but I can't find my notes on this one, so all I've got to go off is this forum thread, where post #3 says I got 1.088 (I always use Refractometer Calculator - Brewer's Friend with a 1.04 wcf). Anyways, it was a DME extract batch, and I'm quite certain the "miss" was adding too much top-off water.


i meant if you take a gravity AND BRIX reading you can punch it into a calc to get ~OG.... and right now with it finishing at 1.015, if the wort did start at 1.088, the refrac should read 10.5 now?
 

bracconiere

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Correct, hydro said 1.015, refractometer reads roughly halfway between 10 and 11 brix.


so, 1.088 was the OG then....


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