Chloropenols

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reinstone

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Had an issue with forgetting to treat sparge water with Camden tablets. How long will it take to detect the off flavors from this? They aren't there pre ferment, will they show up later? Thanks
 
They show up post-ferment. It's caused by the phenol compounds produced by the yeast interacting with the chlorine. They don't show up in wort, as the phenols aren't yet there from the yeast.
 
All depends on your water, chlorine or chloromine, and the levels of them. I couldn't tell in a pale ale till bottling. A black ipa until after conditioning. Then I started using campden. I guess the lighter the quicker?
 
They show up post-ferment. It's caused by the phenol compounds produced by the yeast interacting with the chlorine. They don't show up in wort, as the phenols aren't yet there from the yeast.

I added a tab to the boil also......

I'm wondering if some of the Camden was still in solution as I added water to the already treated water to sparge. Thanks
 
I added a tab to the boil also......

I'm wondering if some of the Camden was still in solution as I added water to the already treated water to sparge. Thanks

Adding campden to the boil won't impact the chlorine/chloramine levels- it has to be done pre-mash for the reaction to occur. The reaction happens quickly, and nothing stays in solution.
 
I added a tab to the boil also......

I'm wondering if some of the Camden was still in solution as I added water to the already treated water to sparge. Thanks

Please see my post Camden issues. Thanks. This has more info on the problem.
 
Adding campden to the boil won't impact the chlorine/chloramine levels- it has to be done pre-mash for the reaction to occur. The reaction happens quickly, and nothing stays in solution.

Dang. And thanks. I guess I'll hop the hops of the ipa cover it up or for some other miracle, I'll report back. I am serving this for a party. Considering a re brew.
 
Adding campden to the boil won't impact the chlorine/chloramine levels- it has to be done pre-mash for the reaction to occur. The reaction happens quickly, and nothing stays in solution.

What happens to the metabisulfate that doesn't react in this case?
 
What happens to the metabisulfate that doesn't react in this case?

It dissipates rather quickly, so it would just go out into the air. I'm not sure how fast it would dissipate in a boil, as I've never boiled a wort or must with sulfites in it- but I know just stirring helps it dissipates quickly so maybe it would dissipate faster in a boil? I dunno.
 
It dissipates rather quickly, so it would just go out into the air. I'm not sure how fast it would dissipate in a boil, as I've never boiled a wort or must with sulfites in it- but I know just stirring helps it dissipates quickly so maybe it would dissipate faster in a boil? I dunno.

Thanks. I'll post back with the results. I'm a fairly harsh judge of my beers I was hoping that because I had the five or so gallons of water that was camden treated when I topped off with tap water that some of the Camden would still have been there to get rid of the chloromine. My water tastes good out of the tap without a noticeable clorine taste so maybe if the planets align this beer won't taste like an electrical fire. First time I ever made this mistake so I'm pissed at myself, guarantee it won't happen again.

I have read about people using a titration of metabisulfate so I'm not sure if they are mislead or I am crazy. Just looking for an out here.

Yoop, do you think I will be able to taste the phenols after primary? If they are there I can dump this batch and brew another.

Time to go back to my checklist on brew day.
Thanks.
 
Thanks. I'll post back with the results. I'm a fairly harsh judge of my beers I was hoping that because I had the five or so gallons of water that was camden treated when I topped off with tap water that some of the Camden would still have been there to get rid of the chloromine. My water tastes good out of the tap without a noticeable clorine taste so maybe if the planets align this beer won't taste like an electrical fire. First time I ever made this mistake so I'm pissed at myself, guarantee it won't happen again.

I have read about people using a titration of metabisulfate so I'm not sure if they are mislead or I am crazy. Just looking for an out here.

Yoop, do you think I will be able to taste the phenols after primary? If they are there I can dump this batch and brew another.

Time to go back to my checklist on brew day.
Thanks.

The water must be treated before the mash in order to avoid chlorophenols. It's ineffective after that. The good news is that since most of your water was treated, and maybe your sparge water stood long enough to off-gas if it was chlorine in the water (not chloramines, which won't boil off or dissipate).

If you do develop chlorophenols, you will be able to taste them after primary.
 
Update. Primary is over, I have tasted the beer and do not taste band aids or an electrical fire. I just taste green beer.

Of course, the phenols could show up at some point but I think I'm gonna go to the keg for dry hops.

I'll update when the beer Is finished . Thanks for all the help here.
 
Good luck. Chloramine is my arch nemesis, every time I add campen to my liqour tank, I pretend I am lex Luther drowning superman in kryptonite.

What? Not every kid good grows up wanting to be a superHERO
Joker-Child-Dark-Knight-Shooting-Illuminati.jpg
 
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