Diacetyl in bottle from keg tranfer

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zodiak3000

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i have been bottling from the keg using the method below. good results except after about 1-2 months i get diacetyl. basically i cant age beers or enter comps using this method if the beer is sitting for 1-2 months. anybody else have this problem? should i just get a blichmann beer gun?


 
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Do you bottle it all or do you have some left in the keg? If you have some left in the keg, does it taste the same as the bottled ones?
 
i just bottle when needed. i had a bottle last night from over a month ago when i did a transfer. butterscotch drain pour. i just killed that same keg last week and the last pints off the draft were tasting excellent.
 
Diacetyl is produced during fermentation. Usually you get diacetyl when pitching unhealth yeast or not enough healthy yeast and also from not aerating enough. If you let the beer sit on the yeast cake, that should typically clean it up. It is odd that you don't taste it in the keg but taste it in bottles from that keg.

I guess it is possible to be from oxidation but I would think that would be more when the beer is on the yeast cake and not racked off into a keg.
 
yeast health and pitching rate are not an issue. aeration is not an issue. i always do a diacetyl rest. the beers taste great in the bottle up to about 1 month. somewhere between 1-2 months something happens where they turn to butterscotch in the bottle.
 
Do a diacetyl test. It's easy. Take two samples of beer. Heat one sample to about 140 or so for an hour. Don't use a microwave. You have to cover the sample with foil or something, when heating. Keep the other sample at room temp or cool it down a little. After the sample is heated, cool it down to the same temp as the other sample. Then smell and taste it. If it smells like butter, you got diacetyl. Then there's no need of the other sample. If it doesn't smell like butter, taste it and compare the taste to the other sample. If they taste different. The yeast isn't done working. I brew mainly tri-decoctioned Pils. My diacetyl rest can be as short as 3 days and as long as four weeks. It all depends on the yeast and a few other things. Anyone saying that a 3-5 day diacetyl rest is long enough, isn't always correct. Especially, when using certain German or Slovak yeast strains. One reason that the beer in a keg doesn't taste like diacetyl as often. Is because the beer was racked into it too early. The hydrometer reading remained stable. So, you figured it was time to keg. However, the yeast became dormant. The yeast, being dormant, didn't knock out the alpha stuff, that it breaks down into diacetyl. Then, the keg is chilled down. Ensuring, that the yeast won't do anything. The yeast, never was in a condition to break down the alpha crap, into diacetyl. Then, when you bottle the beer. The yeast gets roused up, the residual yeast warms up a little and begins working on the alpha thing, while in the bottle. After aging in the bottle, Bingo, diacetyl. Sometimes doing the secondary thing isn't a bad idea. Transfering to a secondary can rouse up the yeast. That's the time when it can break down the alpha jiggers to diacetyl. If you have real good yeast and leave it in the primary for a few weeks, hopefully the yeast will break down the alpha stuff into diacetyl. Then, a diacetyl rest can remove the diacetyl. There's only one time I use an hydrometer during the brewing process, thats for knowing the Grav after cooling. I'm not big in the ABV wonder world. After that, I use a sugar test kit and a pH meter. If I discover a high level of fermentable sugar in the beer after a few weeks in the fermenter and if the pH isn't right for the yeast I use. Then the yeast needs rousing. If that doesn't work. I add more yeast when the starter is in high krausen. The high ferment temps of an ale should eliminate diacetyl. If it doesn't, I'd think that the yeast is crappy or the ferment temps weren't right. I'm assuming your making Lager or Pils.
 
bump, anyone else have this problem or got advice?

Where are you storing the bottles? Room temp? Or in the fridge? If you're storing them warm, maybe that's the problem? Seems more likely that whatever you're using to transfer is contaminating it somehow.
 
Do a diacetyl test. It's easy. Take two samples of beer. Heat one sample to about 140 or so for an hour. Don't use a microwave. You have to cover the sample with foil or something, when heating. Keep the other sample at room temp or cool it down a little. After the sample is heated, cool it down to the same temp as the other sample. Then smell and taste it. If it smells like butter, you got diacetyl. Then there's no need of the other sample. If it doesn't smell like butter, taste it and compare the taste to the other sample. If they taste different. The yeast isn't done working. I brew mainly tri-decoctioned Pils. My diacetyl rest can be as short as 3 days and as long as four weeks. It all depends on the yeast and a few other things. Anyone saying that a 3-5 day diacetyl rest is long enough, isn't always correct. Especially, when using certain German or Slovak yeast strains. One reason that the beer in a keg doesn't taste like diacetyl as often. Is because the beer was racked into it too early. The hydrometer reading remained stable. So, you figured it was time to keg. However, the yeast became dormant. The yeast, being dormant, didn't knock out the alpha stuff, that it breaks down into diacetyl. Then, the keg is chilled down. Ensuring, that the yeast won't do anything. The yeast, never was in a condition to break down the alpha crap, into diacetyl. Then, when you bottle the beer. The yeast gets roused up, the residual yeast warms up a little and begins working on the alpha thing, while in the bottle. After aging in the bottle, Bingo, diacetyl. Sometimes doing the secondary thing isn't a bad idea. Transfering to a secondary can rouse up the yeast. That's the time when it can break down the alpha jiggers to diacetyl. If you have real good yeast and leave it in the primary for a few weeks, hopefully the yeast will break down the alpha stuff into diacetyl. Then, a diacetyl rest can remove the diacetyl. There's only one time I use an hydrometer during the brewing process, thats for knowing the Grav after cooling. I'm not big in the ABV wonder world. After that, I use a sugar test kit and a pH meter. If I discover a high level of fermentable sugar in the beer after a few weeks in the fermenter and if the pH isn't right for the yeast I use. Then the yeast needs rousing. If that doesn't work. I add more yeast when the starter is in high krausen. The high ferment temps of an ale should eliminate diacetyl. If it doesn't, I'd think that the yeast is crappy or the ferment temps weren't right. I'm assuming your making Lager or Pils.

thanks for the response. i ferment in primary only, temp controlled. i brew mostly ales. i always make proper starters via mrmalty.com. the IPA was in for 23 days (plenty of time to clean up). im still not convinced i encountered this off-flavor (diacetyl or not) from fermentation. i feel its some form of oxidation but i might be wrong. the butterscotch flavor just resembles the description of diacetyl.
 
Where are you storing the bottles? Room temp? Or in the fridge? If you're storing them warm, maybe that's the problem? Seems more likely that whatever you're using to transfer is contaminating it somehow.

i think you might be right about this part. bottles are always stored in fridge. i stored these ones on there side though. maybe that caused oxidation? everything is sanitized with starsan from a spray bottle so im not sure. i spray the bottles down then put them in the freezer till they are chilled. maybe im catching something in the freezer?
 
I've never heard oxidation causing a butterscotch flavor. Oxidation is usually cadrboard like. Butterscotch is usually diacetyl which is an off flavor of fermentation.
 
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