 |
|
01-03-2012, 03:27 PM
|
#1
|
|
Frau Administrator
Feedback Score: 0 reviews
Join Date: Jun 2006
Location: Upper Michigan
Posts: 51,683
Liked 1961 Times on 1504 Posts Likes Given: 89
|
pH meter questions
|
|
I got a Milwaukee ph56 for Christmas. It seems simple enough, so I feel funny asking questions, but I can't find the answer on the Milwaukee website.
When I calibrate, the first three or four times I try, I get "wrng" as a message when I move to the 4.01 buffer solution. It does seem to calibrate, though. After a few times of attempting, it does work. This just doesn't seem right to me at all.
The next thing is it takes a really long time to "lock in" to a pH. I mean, a really long time. The instructions say to gently stir, and that seems to speed it up. But it takes several minutes, moving very slowly to go to a pH and settle.
When I left it sitting in the 4.01 buffer, (the instructions say you can), the pH reading eventually dropped to 3.89. That's a big difference! Is that supposed to happen- it seems like if the 4.01 buffer is 4.01, that the meter wouldn't read differently!
__________________
Broken Leg Brewery
Giving beer a leg to stand on since 2006
|
|
|
01-03-2012, 04:27 PM
|
#2
|
|
Feedback Score: 1 reviews
Join Date: Aug 2008
Location: Portland OR
Posts: 5,420
Liked 48 Times on 46 Posts Likes Given: 29
|
I believe the buffers are going to change as they sit out in the atmosphere. Don't know how long that takes. Also temperature correction plays a part - not sure if your meter corrects or not. The packet of solution I have has a temp correction chart on it. I have a super cheap PH meter and it doesn't take very long for it to settle on a number, not sure if it is a correct number but it makes me feel better.
|
|
|
01-03-2012, 04:31 PM
|
#3
|
|
Frau Administrator
Feedback Score: 0 reviews
Join Date: Jun 2006
Location: Upper Michigan
Posts: 51,683
Liked 1961 Times on 1504 Posts Likes Given: 89
|
Quote:
Originally Posted by samc
I believe the buffers are going to change as they sit out in the atmosphere. Don't know how long that takes. Also temperature correction plays a part - not sure if your meter corrects or not. The packet of solution I have has a temp correction chart on it. I have a super cheap PH meter and it doesn't take very long for it to settle on a number, not sure if it is a correct number but it makes me feel better.
|
I emailed the company, and heard back once and answered their questions.
I'm inclined to believe the probe is defective, as I calibrated and checked the pH of my wort (all at 68 degrees, even though the meter supposedly has ATC). The pH took FOREVER but finally stabilized at 5.40. Then I dipped it in water just to rinse a bit and stuck it back in the 4.01 buffer. (I just took it OUT of there before checking the wort pH). It read 3.81. I put fresh solution in both containers, recalibrated, and checked my wort. It read 5.2.
So, which IS the pH of my wort? 5.2? 5.4? None of the above?
I calibrated this thing about 5 times today and never got the same reading twice.
__________________
Broken Leg Brewery
Giving beer a leg to stand on since 2006
|
|
|
01-03-2012, 05:17 PM
|
#4
|
|
Feedback Score: 0 reviews
Join Date: May 2011
Location: Gardner, Kansas
Posts: 70
|
I've never used Milwaukee PH meter for brewing but I used to have one for a Calcium reactor for reef tank and I went through 2 probes when meter was brand new before the 3rd one was good. Maybe it is a defective probe.
Here is contact info:
Milwaukee Instruments, Inc.
2950 Business Park Drive
Rocky Mount, NC 27804 - U.S.A.
Tel.: +1.252.443.3630
Fax: +1.252.443.1937
Primary: milwaukee@vol.com
Sales Dept: sales@milwaukeeinstruments.com
Technical Dept: support@milwaukeeinstruments.com
|
|
|
01-03-2012, 05:51 PM
|
#5
|
|
Frau Administrator
Feedback Score: 0 reviews
Join Date: Jun 2006
Location: Upper Michigan
Posts: 51,683
Liked 1961 Times on 1504 Posts Likes Given: 89
|
They've already emailed me back and are sending out a new replacement probe. It must be defective.
That's great, except I can't brew again until the end of March so I won't even know if it's working properly. Well, I can take the pH of my finished beers, I guess.
__________________
Broken Leg Brewery
Giving beer a leg to stand on since 2006
|
|
|
01-08-2012, 03:58 AM
|
#6
|
|
Electric AG Brewer
Feedback Score: 0 reviews
Join Date: Jan 2011
Location: Monroe, WI
Posts: 103
Liked 3 Times on 3 Posts Likes Given: 3
|
I use a Hanna pH meter at work several times a day, every day. It is usually pretty fast and accurate in spite of being a few years old. I calibrate it every couple of weeks. It gets a little stubborn sometimes when calibrating so I "re-boot" it by taking the batteries out. They probably don't really need it but I clean the batteries when I take them out. After returning the batteries, I clean the probe with a cotton swab and water. The meter is stored in a glass of tap water every day, all day.
If your meter acts up again, even with the new probe, try the re-boot trick. It may help, it may not. Nothing ventured, nothing gained.
__________________
Rocket Socks Brewery
|
|
|
01-08-2012, 03:30 PM
|
#7
|
|
Frau Administrator
Feedback Score: 0 reviews
Join Date: Jun 2006
Location: Upper Michigan
Posts: 51,683
Liked 1961 Times on 1504 Posts Likes Given: 89
|
Quote:
Originally Posted by skipper1953
I use a Hanna pH meter at work several times a day, every day. It is usually pretty fast and accurate in spite of being a few years old. I calibrate it every couple of weeks. It gets a little stubborn sometimes when calibrating so I "re-boot" it by taking the batteries out. They probably don't really need it but I clean the batteries when I take them out. After returning the batteries, I clean the probe with a cotton swab and water. The meter is stored in a glass of tap water every day, all day.
If your meter acts up again, even with the new probe, try the re-boot trick. It may help, it may not. Nothing ventured, nothing gained.
|
Thanks! I have the new probe soaking in storage solution now, and I'll calibrate it tonight. I'm not brewing for a while, but I can check pH of several wines I guess, for practice!
I have another question, then- what is the "instability indicator"? I see no mention of it in the manual.
__________________
Broken Leg Brewery
Giving beer a leg to stand on since 2006
|
|
|
01-08-2012, 04:49 PM
|
#8
|
|
Feedback Score: 0 reviews
Join Date: Nov 2009
Location: Alternate Universe
Posts: 1,995
Liked 35 Times on 33 Posts Likes Given: 8
|
Quote:
Originally Posted by Yooper
I have another question, then- what is the "instability indicator"? I see no mention of it in the manual.
|
You can safely ignore that for now as I have no plans on visiting the UP anytime soon.
|
|
|
01-08-2012, 05:03 PM
|
#9
|
|
Feedback Score: 0 reviews
Join Date: Nov 2011
Location: Sammamish, WA
Posts: 384
Liked 8 Times on 7 Posts
|
Quote:
Originally Posted by skipper1953
I use a Hanna pH meter at work several times a day, every day. It is usually pretty fast and accurate in spite of being a few years old. I calibrate it every couple of weeks. It gets a little stubborn sometimes when calibrating so I "re-boot" it by taking the batteries out. They probably don't really need it but I clean the batteries when I take them out. After returning the batteries, I clean the probe with a cotton swab and water. The meter is stored in a glass of tap water every day, all day.
If your meter acts up again, even with the new probe, try the re-boot trick. It may help, it may not. Nothing ventured, nothing gained.
|
Hey Skipper,
Just curious on you storing the probe in tap water - is that just as effective as that storage solution they sell? Curious as I'm looking at purchasing the Hanna pHep 5 from MoreBeer!
Thanks
|
|
|
01-09-2012, 12:34 AM
|
#10
|
|
Electric AG Brewer
Feedback Score: 0 reviews
Join Date: Jan 2011
Location: Monroe, WI
Posts: 103
Liked 3 Times on 3 Posts Likes Given: 3
|
Quote:
Originally Posted by jholen
Hey Skipper,
Just curious on you storing the probe in tap water - is that just as effective as that storage solution they sell? Curious as I'm looking at purchasing the Hanna pHep 5 from MoreBeer!
Thanks
|
I don't require a high degree of accuracy from my meter. The way I handle and store my meter probably reflects that fact. I honestly don't know if my system is as effective as following the manufacturers instructions. It works for me.
I use the Hanna meter for testing the pH of industrial waste water while batch processing. After testing the pH of a water sample, I rinse the probe with a garden hose and stick it in a plastic beaker half full of clean tap water. I have not changed the replaceable glass portion of the meter for a couple of years but I think I'm about due. Before calibrating, I usually check the pH of the 7.0 buffer solution just for the sake of curiosity. The meter is not usually off by much and when it is it is usually a bit high (7.5ish at most).
My own meter (the one I use for brewing and wine making) is stored with a bit of wet (tap water) cotton in the cap. I wrap electrical tape around the cap to seal in the moisture. When I use the meter, I soak it in water while I'm getting things ready. I do a two step calibration using 7.0 and 4.0 buffer solutions before use to insure accuracy. I've had my Hanna meter for several years and I am still using the original glass probe.
I'm satisfied that I don't need to buy a special storage solution. Your mileage may vary.
__________________
Rocket Socks Brewery
|
|
|
| Thread Tools |
|
|
| Display Modes |
Linear Mode
|
Similar Threads
|
| Thread |
Thread Starter |
Forum |
Replies |
Last Post |
|
pH meter
|
amrmedic |
Equipment/Sanitation |
3 |
03-22-2011 05:43 PM |
|
Ph meter
|
Hugh_Jass |
Equipment/Sanitation |
26 |
01-07-2010 09:06 PM |
|
Questions about ph Meter
|
GroosBrewz |
Equipment/Sanitation |
6 |
03-10-2009 02:08 AM |
|
Vin-O-Meter
|
bkov |
Equipment/Sanitation |
1 |
08-16-2008 01:38 PM |
|
Ph meter
|
Dark_Ale |
Equipment/Sanitation |
5 |
07-22-2005 03:44 PM |
|
|
|